3O 391 then FR 5376 at Madrid
Tangier → Madrid → Brussels Charleroi
Timetable, Madrid time
16:403O 391 from Tangier at the gate
09:20FR 5376 to Brussels Charleroi leaves the gate
16 h 40 apart on the timetable, overnight
FR 5376 leaves 16 h 40 after 3O 391 arrives on the timetable: more than half a day, so not a connection we count.